ChemicalBook >> CAS DataBase List >>5-Methoxyindole
5-Methoxyindole
- CAS No.
- 1006-94-6
- Chemical Name:
- 5-Methoxyindole
- Synonyms
- 5-METHOXY-1H-INDOLE;Methoxyindole 99% indol-5-yl methyl ether;5-methoxy-indol;Femedol;NSC 521752;AKOS JY2082918;5-METHOXYINDOLE;methoxy-5indole;5-MethoxyindoleF;Methoxy-5 indole
- CBNumber:
- CB4223553
- Molecular Formula:
- C9H9NO
- Molecular Weight:
- 147.17
- MDL Number:
- MFCD00005674
- MOL File:
- 1006-94-6.mol
- MSDS File:
- SDS
Last updated:2023-11-16 17:07:08
| Melting point | 52-55 °C (lit.) |
|---|---|
| Boiling point | 176-178 °C/17 mmHg (lit.) |
| Density | 1.1135 (rough estimate) |
| refractive index | 1.5310 (estimate) |
| Flash point | 176-178°C/17mm |
| storage temp. | Keep in dark place,Sealed in dry,Room Temperature |
| solubility | Chloroform, Methanol |
| form | Crystalline Powder |
| pka | 16.70±0.30(Predicted) |
| color | White to light brownish |
| Water Solubility | insoluble |
| Sensitive | Light Sensitive |
| BRN | 116722 |
| InChIKey | DWAQDRSOVMLGRQ-UHFFFAOYSA-N |
| CAS DataBase Reference | 1006-94-6(CAS DataBase Reference) |
| EWG's Food Scores | 1 |
| FDA UNII | DQM3AS43PQ |
| NIST Chemistry Reference | 1H-Indole, 5-methoxy-(1006-94-6) |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|||||||||
|---|---|---|---|---|---|---|---|---|---|---|
| Signal word | Warning | |||||||||
| Hazard statements | H315-H319-H335 | |||||||||
| Precautionary statements | P261-P264-P271-P280-P302+P352-P305+P351+P338 | |||||||||
| Hazard Codes | Xi | |||||||||
| Risk Statements | 36/37/38 | |||||||||
| Safety Statements | 26-36-24/25-37/39 | |||||||||
| WGK Germany | 3 | |||||||||
| RTECS | NL9500000 | |||||||||
| F | 8 | |||||||||
| Hazard Note | Irritant | |||||||||
| HazardClass | IRRITANT, KEEP COLD, LIGHT SENSITIVE | |||||||||
| HS Code | 29339900 | |||||||||
| NFPA 704 |
|
5-Methoxyindole price More Price(31)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Sigma-Aldrich | M14900 | 5-Methoxyindole 99% | 1006-94-6 | 1g | $25 | 2023-06-20 | Buy |
| Sigma-Aldrich | M14900 | 5-Methoxyindole 99% | 1006-94-6 | 5g | $34 | 2023-06-20 | Buy |
| TCI Chemical | M0731 | 5-Methoxyindole >99.0%(GC) | 1006-94-6 | 1g | $32 | 2023-06-20 | Buy |
| TCI Chemical | M0731 | 5-Methoxyindole >99.0%(GC) | 1006-94-6 | 5g | $55 | 2023-06-20 | Buy |
| Alfa Aesar | B25290 | 5-Methoxyindole, 99% | 1006-94-6 | 1g | $41 | 2023-06-20 | Buy |
5-Methoxyindole Chemical Properties,Uses,Production
Chemical Properties
white to light brownish crystalline powder
Uses
5-Methoxyindole (cas# 1006-94-6) is a compound useful in organic synthesis. It can be used to synthesis 1-(Phenylsulfonyl)-5-methoxy-1H-indole.
Definition
ChEBI: 5-methoxyindole is a member of indoles.
Preparation
The synthesis of 5-methoxyindole from 5-methoxy-2-oxindole: Conversion of 5-methoxy-2-oxindole to 5-methoxyindole was accomplishedby the chlorination of 5-methoxy-2-oxindole with triphenylphosphine-carbontetrachloride in acetonitrile followed by the catalytic reduction of a chlorine atom in 66% total yield.
Reactions
5-methoxyindole was treated with sodium hydroxide and phenylsulfonyl chloride in the presence of a catalytic amount of tetrabutylammonium bromide to afford 1-(phenylsulfonyl)indole and 5-methoxy-1-(phenylsufonyl)indole in excellent yields of 100%.
Synthesis Reference(s)
Journal of Heterocyclic Chemistry, 26, p. 1405, 1989 DOI: 10.1002/jhet.5570260533
The Journal of Organic Chemistry, 58, p. 5558, 1993 DOI: 10.1021/jo00072a052
Tetrahedron Letters, 27, p. 837, 1986 DOI: 10.1016/S0040-4039(00)84114-3
Purification Methods
Crystallise 5-methoxyindole from cyclohexane pet ether or pet ether/Et2O. [Saito & Kikugawa J Heterocycl Chem 16 1325 1979, Beilstein 21 III/IV 765, 21/3 V 18.]
5-Methoxyindole Preparation Products And Raw materials
Raw materials
EthenaMine, 2-(5-Methoxy-2-nitrophenyl)-N,N-diMethyl-, (1E)-
1-Propanone, 1-(5-methoxy-1H-indol-1-yl)-2,2-dimethyl-
Benzene, 2-ethenyl-4-methoxy-1-nitro-
5-Methoxyindole-3-carboxaldehyde
Phosphonium, [2-(1,1-dimethylethoxy)-2-oxoethyl]triphenyl-, inner salt
1of3
Preparation Products
Global( 569)Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Shanghai UCHEM Inc. | +862156762820 +86-13564624040 | sales@myuchem.com | China | 6076 | 58 |
| Capot Chemical Co.,Ltd. | 571-85586718 +8613336195806 | sales@capotchem.com | China | 29767 | 60 |
| Henan Tianfu Chemical Co.,Ltd. | +86-0371-55170693 +86-19937530512 | info@tianfuchem.com | China | 21722 | 55 |
| ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 | ivan@atkchemical.com | China | 32237 | 60 |
| career henan chemical co | +86-0371-86658258 | sales@coreychem.com | China | 29922 | 58 |
| Zhejiang ZETian Fine Chemicals Co. LTD | 18957127338 | stella@zetchem.com | China | 2141 | 58 |
| Hubei Jusheng Technology Co.,Ltd. | 18871490254 | linda@hubeijusheng.com | CHINA | 28183 | 58 |
| Hebei Guanlang Biotechnology Co., Ltd. | +86-19930503282 | alice@crovellbio.com | China | 8836 | 58 |
| Changzhou Ditong Chemical Co.,Ltd | +86-0519-88299272 | info@edengenechem.com | China | 2169 | 58 |
| Shandong chuangyingchemical Co., Ltd. | 18853181302 | sale@chuangyingchem.com | CHINA | 5911 | 58 |
View Lastest Price from 5-Methoxyindole manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2023-11-16 | 5-Methoxyindole
1006-94-6
|
US $129.00-645.00 / g | 1g | 0.99 | 25kg | Shanghai UCHEM Inc. | |
 |
2023-07-25 | 5-Methoxyindole
1006-94-6
|
US $20.00-10.00 / kg | 1kg | 99% | 2T | Hebei Yanxi Chemical Co., Ltd. | |
 |
2023-03-27 | 5-Methoxyindole
1006-94-6
|
US $25.00 / KG | 1KG | 0.99 | 5000KG/MONTH | XINGTAI XINGJIU NEW MATERIAL TECHNOLOGY CO., LTD |
-
- 5-Methoxyindole
1006-94-6
- US $129.00-645.00 / g
- 0.99
- Shanghai UCHEM Inc.
-
- 5-Methoxyindole
1006-94-6
- US $20.00-10.00 / kg
- 99%
- Hebei Yanxi Chemical Co., Ltd.
-
- 5-Methoxyindole
1006-94-6
- US $25.00 / KG
- 0.99
- XINGTAI XINGJIU NEW MATERIAL TECHNOLOGY CO., LTD
1006-94-6(5-Methoxyindole)Related Search:
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5-Methoxyindole in stock Factory
5-Methoxyindole>
5-Methoxyindole 1006-94-6
Methoxyindole 99% indol-5-yl methyl ether
5-METHOXY-1H-INDOLE
5-methoxy-indol
1006-94-6
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